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Forskar­utbildnings­kurser

Faculty of Engineering | Lund University

Detaljer för kursplan för kurs KAS025F giltig från och med Spring 2023

Utskriftsvänlig visning

Allmänt
Syfte
  • There is no course for doctoral students that covers NMR spectroscopy without extensive mathematics. This course fulfils a long-awaited need for chemists who use NMR spectroscopy but do not require the quantum chemical background provided in the KFKN01F course.
Innehåll
  • The aim is to provide fundamental knowledge in nuclear magnetic resonance (NMR) and a solid understanding of how the technique can be employed to study the structure and dynamics of small molecules. The course covers methods focused on organic and organometallic molecules.
    The course begins with the fundamental theory of nuclear magnetic resonance. It is followed by lectures on chemical shift, nuclear spin interactions, spin dynamics, chemical exchange, relaxation, and multidimensional applications. Finally, each student completes a project where a molecule's structure is studied using various NMR methods. The focus of this project may vary depending on the student's specialization.
Kunskap och förståelse
  • För godkänd kurs skall doktoranden
  • Understand and explain the basic principles of nuclear magnetic resonance spectroscopy (NMR spectroscopy), including a vector-based description of NMR pulses.
    Have knowledge of how nuclear magnetic resonance can be used to study the dynamics of molecules.
    Have knowledge of the most common multidimensional NMR experiments and the principles of their use in determining the structures of organic and organometallic molecules.
Färdighet och förmåga
  • För godkänd kurs skall doktoranden
  • Calibrate and optimize the common parameters in pulse sequences.
    Interpret information from the most common one- and multidimensional NMR experiments.
    Describe a molecule's dynamic and structural properties based on NMR data.
    Independently perform NMR experiments with limited guidance.
    Clearly present results and interpretations of NMR experiments both orally and in writing.
Värderingsförmåga och förhållningssätt
  • För godkänd kurs skall doktoranden
  • Choose the NMR technique that is best suited for studying a given structural or dynamic problem.
Undervisningsformer
  • Föreläsningar
  • Seminarier
  • övningar
  • Projekt
  • Participation in exercises and seminars is mandatory.
Examinationsformer
  • Skriftlig tentamen
  • Skriftlig rapport
  • Inlämningsuppgifter
  • Seminarieföredrag av deltagarna
  • Underkänd, godkänd
Förkunskapskrav
Förutsatta förkunskaper
  • Master degree knowledge of inorganic and organic chemistry
Urvalskriterier
Litteratur
  • Claridge, Timothy D.W.: High-Resolution NMR Techniques in Organic Chemistry. Elsevier Science.
Övrig information
  • At least 5 students needed
Kurskod
  • KAS025F
Administrativ information
  • 2024-04-09
  • Jens Wahlström

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